Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

Base Information

Chemical Name:Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate
CAS No.:943124-70-7
Molecular Formula:C₂₅H₂₆N₂O₂Se
Molecular Weight:465.454
Hs Code.:

Synonyms:Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

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Chemical Property of Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

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Technology Process of Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

There total 5 articles about Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₂N₂O₂

: 943124-70-7
Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: LiOH*H₂O / tetrahydrofuran; H₂O / 5 h / 65 °C

3: Et₃N; tributylphosphine / CH₂Cl₂; tetrahydrofuran

With lithium hydroxide; tributylphosphine; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo070322m

Reference yield:

: 943124-61-6
methyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboxylate

: 943124-70-7
Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

Guidance literature:: Multi-step reaction with 2 steps

1: LiOH*H₂O / tetrahydrofuran; H₂O / 5 h / 65 °C

2: Et₃N; tributylphosphine / CH₂Cl₂; tetrahydrofuran

With lithium hydroxide; tributylphosphine; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo070322m

Reference yield:

: 1541-25-9
3-amino-1-cyclohexene

: 943124-70-7
Se-phenyl 3-[N-acetyl-N-(2-cyclohexenyl)aminomethyl]-1-methylindole-2-carboselenoate

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH(AcO)3; AcOH / CH₂Cl₂ / 12 h / 20 °C

2: Et₃N / CH₂Cl₂ / 20 °C

3: LiOH*H₂O / tetrahydrofuran; H₂O / 5 h / 65 °C

4: Et₃N; tributylphosphine / CH₂Cl₂; tetrahydrofuran

With lithium hydroxide; tributylphosphine; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo070322m