N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

Base Information

Chemical Name:N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide
CAS No.:120791-49-3
Molecular Formula:C₁₉H₂₀N₂O₂
Molecular Weight:308.38
Hs Code.:

Synonyms:N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

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Chemical Property of N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

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Technology Process of N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

There total 5 articles about N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100510-64-3
1,3-Dihydro-3,3-dimethyl-6-nitro-2H-indol-2-one

: 120791-49-3
N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 70 °C

2: 57.8 g / hydrogen / 10 percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

3: 68.7 g / toluene / 4 h / Heating

4: 1.) NaH / 1.) DMSO, 30 min

With hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00127a015

Reference yield:

: 100-44-7
benzyl chloride

: 120791-49-3
N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 70 °C

2: 57.8 g / hydrogen / 10 percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

3: 68.7 g / toluene / 4 h / Heating

4: 1.) NaH / 1.) DMSO, 30 min

With hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00127a015

Reference yield:

: 120791-47-1
1-Benzyl-1,3-dihydro-3,3-dimethyl-6-nitro-2H-indol-2-one

: 120791-49-3
N-Methyl-N-(1-benzyl-1,3-dihydro-3,3-dimethyl-2-oxo-2H-6-indolyl)formamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57.8 g / hydrogen / 10 percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

2: 68.7 g / toluene / 4 h / Heating

3: 1.) NaH / 1.) DMSO, 30 min

With hydrogen; sodium hydride; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jm00127a015