N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester

Base Information

• Chemical Name: N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester
• CAS No.: 515164-50-8
• Molecular Formula: C₂₃H₃₁N₃O₅
• Molecular Weight: 429.516

Synonyms:N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester

Chemical Property of N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester

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Technology Process of N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester

There total 1 articles about N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

2-methylpropyl(methyl)amine (625-43-4) + N-(5-(3-bromophenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester (515164-49-5) → N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester (515164-50-8)

Guidance literature:

With potassium tert-butylate; CyJohnPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 100 ℃; for 1.5h;

Reference yield: 77.0%

N-(5-(3-(isobutyl-methyl-amino)phenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester (515164-50-8) → N-(2-amino-5-(3-(isobutyl-methyl-amino)phenoxy)-phenyl)-N-methylcarbamic acid t-butyl ester (515164-51-9)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 2.5h;

upstream raw materials:

2-methylpropyl(methyl)amine

N-(5-(3-bromophenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester

Downstream raw materials:

N-(2-amino-5-(3-(isobutyl-methyl-amino)phenoxy)-phenyl)-N-methylcarbamic acid t-butyl ester

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