C₂HF₃O₂*C₁₃H₁₅N₃O₇S

Base Information

• Chemical Name: C₂HF₃O₂*C₁₃H₁₅N₃O₇S
• CAS No.: 1236359-08-2
• Molecular Formula: C₂HF₃O₂*C₁₃H₁₅N₃O₇S
• Molecular Weight: 471.368
• Mol file: 1236359-08-2.mol

Synonyms:C₂HF₃O₂*C₁₃H₁₅N₃O₇S

Chemical Property of C₂HF₃O₂*C₁₃H₁₅N₃O₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂HF₃O₂*C₁₃H₁₅N₃O₇S

There total 3 articles about C₂HF₃O₂*C₁₃H₁₅N₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H23N3O9S (1236359-05-9) + trifluoroacetic acid (76-05-1) → C2HF3O2*C13H15N3O7S (1236359-08-2)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2010.09.070

Reference yield:

3-(4-benzenesulfonyl-5-oxy-furazan-3-yloxy)-propan-1-ol (361541-87-9) → C2HF3O2*C13H15N3O7S (1236359-08-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C

2: dichloromethane / 20 °C / Cooling

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1016/j.cclet.2015.04.002

Reference yield:

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (66074-00-8) → C2HF3O2*C13H15N3O7S (1236359-08-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / tetrahydrofuran; water / 20 °C / Cooling

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C

3: dichloromethane / 20 °C / Cooling

With dmap; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;

DOI:10.1016/j.cclet.2015.04.002

upstream raw materials:

C₁₈H₂₃N₃O₉S

trifluoroacetic acid

3-(4-benzenesulfonyl-5-oxy-furazan-3-yloxy)-propan-1-ol

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

Downstream raw materials:

C₄₃H₅₉N₃O₁₀S