methyl [methyl(dimethylphosphonate)]phenyl phosphinate

Base Information

Chemical Name:methyl [methyl(dimethylphosphonate)]phenyl phosphinate
CAS No.:1382937-02-1
Molecular Formula:C₁₀H₁₆O₅P₂
Molecular Weight:278.182
Hs Code.:

Synonyms:methyl [methyl(dimethylphosphonate)]phenyl phosphinate

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Chemical Property of methyl [methyl(dimethylphosphonate)]phenyl phosphinate

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Technology Process of methyl [methyl(dimethylphosphonate)]phenyl phosphinate

There total 5 articles about methyl [methyl(dimethylphosphonate)]phenyl phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2857-97-8
trimethylsilyl bromide

: 1382937-01-0
butyl [(diisopropylphosphono)methyl]phenyl phosphinate

: 1382937-02-1
methyl [methyl(dimethylphosphonate)]phenyl phosphinate

Guidance literature:: In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol3013793

Reference yield:

: 1382936-98-2
butyl [(tosyloxy)methyl]phenyl phosphinate

: 1382937-02-1
methyl [methyl(dimethylphosphonate)]phenyl phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hydride; In dichloromethane; 1.1: Michaelis-Becker condition / 1.2: Michaelis-Becker condition;
DOI:10.1021/ol3013793

Reference yield:

: 1382936-86-8
butyl (hydroxymethyl)phenyl phosphinate

: 1382937-02-1
methyl [methyl(dimethylphosphonate)]phenyl phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 20 h / 20 °C / Inert atmosphere

3.1: dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; 2.1: Michaelis-Becker condition / 2.2: Michaelis-Becker condition;
DOI:10.1021/ol3013793