octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

Base Information

Chemical Name:octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside
CAS No.:118250-07-0
Molecular Formula:C₇₅H₈₇NO₁₉
Molecular Weight:1306.51
Hs Code.:

octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

Synonyms:octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

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Chemical Property of octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

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Technology Process of octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

There total 11 articles about octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 118250-01-4
(2S,3S,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-((2S,4S,5R,6R)-4,5-bis-benzyloxy-6-octyloxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-3-ol

: 118250-07-0
octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 100-39-0
benzyl bromide

: 118250-07-0
octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

Guidance literature:: Multi-step reaction with 9 steps

1: NaH (60percent, dispersion im oil) / dimethylformamide / 20 h / Ambient temperature

2: 86 percent / aq. 80percent acetic acid / CH₂Cl₂ / 2 h / 80 °C

3: 71.6 percent / pyridine / CH₂Cl₂ / 1) -78 deg C, 3 h: 2) 0 deg C, 1 h

4: 52 percent / 4-dimethylaminopyridine / acetonitrile / 5 h / Heating

5: 91 percent / 2,2'-azobis(isobutyronitrile), tribuylstannane / toluene / 2 h / 80 °C

6: 95 percent / sodium methoxide / methanol / 5 h / Ambient temperature

7: 76 percent / silver trifluoromethanesulfonate, tetramethylurea / CH₂Cl₂ / 2 h

8: 82 percent / sodium methoxide / methanol

9: 74 percent / silver trifluoromethanesulfonate, sym-collidine, molecular sieve (4 Angstroem) / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; dmap; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tri-n-butyl-tin hydride; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; acetic acid; tetramethylurea; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 118249-73-3
n-octyl 4,6-O-benzylidene-β-D-glucopyranoside

: 118250-07-0
octyl 2,3-di-O-benzyl-4-deoxy-6-O-<3,4,6-tri-O-benzyl-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-xylohexopyranoside

Guidance literature:: Multi-step reaction with 9 steps

1: NaH (60percent, dispersion im oil) / dimethylformamide / 20 h / Ambient temperature

2: 86 percent / aq. 80percent acetic acid / CH₂Cl₂ / 2 h / 80 °C

3: 71.6 percent / pyridine / CH₂Cl₂ / 1) -78 deg C, 3 h: 2) 0 deg C, 1 h

4: 52 percent / 4-dimethylaminopyridine / acetonitrile / 5 h / Heating

5: 91 percent / 2,2'-azobis(isobutyronitrile), tribuylstannane / toluene / 2 h / 80 °C

6: 95 percent / sodium methoxide / methanol / 5 h / Ambient temperature

7: 76 percent / silver trifluoromethanesulfonate, tetramethylurea / CH₂Cl₂ / 2 h

8: 82 percent / sodium methoxide / methanol

9: 74 percent / silver trifluoromethanesulfonate, sym-collidine, molecular sieve (4 Angstroem) / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; dmap; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tri-n-butyl-tin hydride; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; acetic acid; tetramethylurea; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/0008-6215(88)84115-6