1-iodo-2-styrylbenzene

Base Information

Chemical Name:1-iodo-2-styrylbenzene
CAS No.:92106-62-2
Molecular Formula:C₁₄H₁₁I
Molecular Weight:306.146
Hs Code.:

Synonyms:1-iodo-2-styrylbenzene

Suppliers and Price of 1-iodo-2-styrylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-iodo-2-styrylbenzene

Chemical Property:

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Technology Process of 1-iodo-2-styrylbenzene

There total 21 articles about 1-iodo-2-styrylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 62680-65-3
(2-iodobenzyl)triphenylphosphonium bromide

: 100-52-7
benzaldehyde

: 92106-62-2
1-iodo-2-styrylbenzene

Guidance literature:: With potassium hydroxide; In chloroform; water; at 20 ℃; for 2.5h; Reflux;

Reference yield: 89.0%

: 26260-02-6
2-iodobenzaldehyde

: 21955-55-5
benzyl(methyl)diphenylphosphonium bromide

: 1138-43-8,5025-41-2,92106-62-2
1-iodo-2-[(Z)-2-phenylethenyl]benzene

Guidance literature:: benzyl(methyl)diphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; for 1h; Inert atmosphere;

2-iodobenzaldehyde; In tetrahydrofuran; at -78 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere; Cooling with acetone-dry ice;
DOI:10.1021/ja300943z

Reference yield: 75.0%

: 26260-02-6
2-iodobenzaldehyde

: 1080-32-6
O,O-diethyl benzylphosphonate

: 5025-41-2,1138-43-8,92106-62-2
1-iodo-2-[(E)-2-phenylethenyl]benzene

Guidance literature:: O,O-diethyl benzylphosphonate; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

2-iodobenzaldehyde; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo501383v