C₃₀H₁₈BrN

Base Information

Chemical Name:C₃₀H₁₈BrN
CAS No.:1421701-40-7
Molecular Formula:C₃₀H₁₈BrN
Molecular Weight:472.384
Hs Code.:

Synonyms:C₃₀H₁₈BrN

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Chemical Property of C₃₀H₁₈BrN

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Technology Process of C₃₀H₁₈BrN

There total 7 articles about C₃₀H₁₈BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.6%

: 1369369-44-7
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)indolo[3,2,1-jk]-carbazole

: 105946-82-5
4-bromo-4'-iodobiphenyl

: 1421701-40-7
C₃₀H₁₈BrN

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In 1,4-dioxane; water; at 100 ℃; for 9h; Inert atmosphere;

Reference yield:

: 6286-72-2
9-(2-nitrophenyl)-9H-carbazole

: 1421701-40-7
C₃₀H₁₈BrN

Guidance literature:: Multi-step reaction with 5 steps

1.1: stannous chloride dihydrate / ethanol / 8 h / 70 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: sulfuric acid; sodium nitrite / water; acetic acid / 0.75 h / 10 - 130 °C / Cooling with ice

3.1: N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

3.2: 13 h

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane; toluene / 17 h / 120 °C / Inert atmosphere

5.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; 1,4-dioxane / 9 h / 100 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; N-Bromosuccinimide; stannous chloride dihydrate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; potassium acetate; potassium carbonate; sodium nitrite; In 1,4-dioxane; ethanol; dichloromethane; water; acetic acid; toluene;

Reference yield:

: 205-95-8
indolo<3,2,1-jk>carbazole

: 1421701-40-7
C₃₀H₁₈BrN

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

1.2: 13 h

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane; toluene / 17 h / 120 °C / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; 1,4-dioxane / 9 h / 100 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In 1,4-dioxane; dichloromethane; water; toluene;