(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

Base Information

Chemical Name:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate
CAS No.:1227514-66-0
Molecular Formula:C₂₉H₃₈Cl₃NO₇Si
Molecular Weight:647.068
Hs Code.:

Synonyms:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

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Chemical Property of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

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Technology Process of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

There total 1 articles about (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1227514-65-9
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 1227514-66-0
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

Guidance literature:: With triethylamine; In diethyl ether; for 1h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tet.2010.02.093

Reference yield: 75.0%

: 1227514-66-0
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl-2,4,6-trichlorobenzoyloxycarbamate

: 1227514-64-8
5-((R)-2-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)butyl)-4-(hydroxymethyl)oxazolidin-2-one

: 5-((R)-2-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)butyl)-4-(hydroxymethyl)oxazolidin-2-one

Guidance literature:: With potassium osmate(VI) dihydrate; water; In tert-butyl alcohol; for 3h; optical yield given as %de;
DOI:10.1016/j.tet.2010.02.093