(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

Base Information

Chemical Name:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate
CAS No.:1227514-65-9
Molecular Formula:C₂₂H₃₇NO₆Si
Molecular Weight:439.624
Hs Code.:

Synonyms:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

Suppliers and Price of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

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Technology Process of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

There total 1 articles about (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1227514-62-6
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-ol

: 1227514-65-9
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)hept-1-en-3-yl hydroxycarbamate

Guidance literature:: (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-ol; With pyridine; 1,1'-carbonyldiimidazole; at 40 ℃; for 4h; Inert atmosphere;

With pyridine; hydroxylamine hydrochloride; at 40 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.093