1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

Base Information

Chemical Name:1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil
CAS No.:41962-40-7
Molecular Formula:C₃₁H₂₇N₃O₈S
Molecular Weight:601.637
Hs Code.:

Synonyms:1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

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Technology Process of 1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

There total 2 articles about 1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.71%

: 31356-85-1
1-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-6-aza-5-methyl-2-thiouracil

: 74-88-4
methyl iodide

: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-6-aza-N³-methyl-5-methyl-2-thiouracil

: 41962-40-7
1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1039/d0nj04154h

Reference yield:

: 50-69-1
D-ribose

: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-6-aza-N³-methyl-5-methyl-2-thiouracil

: 41962-40-7
1-(2,3,5-tri-O-benzoyl-β-D-ribo-furanosyl)-6-aza-5-methyl-2-methylthiouracil

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 5 h / 20 °C

2.1: pyridine / 12 h / 0 - 20 °C

3.1: sulfuric acid / acetic acid / 5 h / 0 - 20 °C

4.1: N,O-bis-(trimethylsilyl)-acetamide / 1,2-dichloro-ethane / 0.5 h / 20 °C

4.2: 3 h / -10 - 0 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1039/d0nj04154h