3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Base Information

• Chemical Name: 3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one
• CAS No.: 209219-68-1
• Molecular Formula: C₁₄H₁₉N₃O₃
• Molecular Weight: 277.323

Synonyms:3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Chemical Property of 3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Chemical Property:

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Technology Process of 3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

There total 1 articles about 3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2(S)-tert-Butoxycarbonylamino-3-(2-nitrophenyl-amino)-propionic acid (209219-69-2) → 3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one (209219-68-1) + 2-tert-butoxycarbonylamino-3-(2-aminophenyl)aminopropionic acid

Guidance literature:

palladium-carbon; In methanol;

Reference yield: 86.9%

3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one (209219-68-1) + benzyl bromide (100-39-0) → 2-oxo-3-tert-butoxycarbonylamino-5-benzyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

Guidance literature:

With sodium hydrogencarbonate; In methanol; water;

Reference yield: 82.0%

3(S)-tert-Butoxycarbonylamino-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one (209219-68-1) + rac-3-bromocyclohexene (1521-51-3,113667-32-6) → 2-oxo-3-tert-butoxycarbonylamino-5-(2-cyclohexen-1-yl)-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

upstream raw materials:

2(S)-tert-Butoxycarbonylamino-3-(2-nitrophenyl-amino)-propionic acid

Downstream raw materials:

2-oxo-3-tert-butoxycarbonylamino-5-[(N-benzyloxycarbonyl)piperidin-2-yl]carbonyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

1-(2-toluoylmethyl)-2-oxo-3-amino-5-(adamantan-1-yl)carbonyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

1-(2-toluoylmethyl)-2-oxo-3-tert-butoxycarbonylamino-5-(adamantan-1-yl)carbonyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

1-[1-(2-toluoylmethyl)-2-oxo-5-(adamantan-1-yl)carbonyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine-3-yl]-3-(3-methylphenyl)urea

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