butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

Base Information

Chemical Name:butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester
CAS No.:1446022-14-5
Molecular Formula:C₁₇H₂₄N₂O₅
Molecular Weight:336.388
Hs Code.:

Synonyms:butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

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Chemical Property of butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

Chemical Property:

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Technology Process of butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

There total 4 articles about butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60456-26-0
(R)-glycidyl butyrate

: 438056-69-0
4-(4-aminophenyl)morpholin-3-one

: 1446022-14-5
butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

Guidance literature:: In ethanol; at 75 - 80 ℃; for 12h;

Reference yield:

: 29518-11-4
4-phenylmorpholin-3-one

: 1446022-14-5
butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 2.5 h / 0 - 5 °C

2: hydrogen; palladium on activated charcoal / dichloromethane / 25 - 80 °C / Inert atmosphere; Autoclave

3: ethanol / 12 h / 75 - 80 °C

With sulfuric acid; palladium on activated charcoal; hydrogen; nitric acid; In ethanol; dichloromethane;

Reference yield:

: 446292-04-2
4-(4-nitrophenyl)-3-morpholinone

: 1446022-14-5
butyric acid-2(R)-2-hydroxy-3-[4-(3-oxo-morpholin-4-yl)phenylamino]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / dichloromethane / 25 - 80 °C / Inert atmosphere; Autoclave

2: ethanol / 12 h / 75 - 80 °C

With palladium on activated charcoal; hydrogen; In ethanol; dichloromethane;