C₁₉H₃₀O₃Si

Base Information

Chemical Name:C₁₉H₃₀O₃Si
CAS No.:1561047-70-8
Molecular Formula:C₁₉H₃₀O₃Si
Molecular Weight:334.531
Hs Code.:

C<sub>19</sub>H<sub>30</sub>O<sub>3</sub>Si

Synonyms:C₁₉H₃₀O₃Si

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Chemical Property of C₁₉H₃₀O₃Si

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Technology Process of C₁₉H₃₀O₃Si

There total 4 articles about C₁₉H₃₀O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-39-0
benzyl bromide

: 101915-61-1
3-O-tert-butyldimethylsilyl-L-fucal

: 1561047-70-8
C₁₉H₃₀O₃Si

Guidance literature:: 3-O-tert-butyldimethylsilyl-L-fucal; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja4116956

Reference yield:

: 73-34-7,87-96-7,488-79-9,551-63-3,609-01-8,643-17-4,643-18-5,4164-09-4,6014-42-2,6155-36-8,6189-71-5,6696-41-9,6736-43-2,13224-93-6,22611-09-2,28161-49-1,28161-50-4,28161-52-6,45864-36-6,63814-64-2,71116-59-1,71116-61-5,72598-05-1,87936-88-7,87936-89-8,97466-79-0,116908-82-8,120442-60-6,123484-22-0,133576-32-6
6-deoxy-L-galactose

: 1561047-70-8
C₁₉H₃₀O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: Acetyl bromide / ethyl acetate / 0.16 h

2.1: zinc / aq. phosphate buffer; ethyl acetate / 0.32 h

3.1: sodium methylate; methanol / N,N-dimethyl-formamide / 0.17 h

4.1: triethylamine; dmap / N,N-dimethyl-formamide / 0.17 h

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.05 h

5.2: 0.11 h

With methanol; dmap; Acetyl bromide; sodium methylate; sodium hexamethyldisilazane; triethylamine; zinc; In tetrahydrofuran; aq. phosphate buffer; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.202109887

Reference yield:

: C₆H₁₁BrO₄

: 1561047-70-8
C₁₉H₃₀O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc / aq. phosphate buffer; ethyl acetate / 0.32 h

2.1: sodium methylate; methanol / N,N-dimethyl-formamide / 0.17 h

3.1: triethylamine; dmap / N,N-dimethyl-formamide / 0.17 h

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.05 h

4.2: 0.11 h

With methanol; dmap; sodium methylate; sodium hexamethyldisilazane; triethylamine; zinc; In tetrahydrofuran; aq. phosphate buffer; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.202109887