10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine

Base Information

• Chemical Name: 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine
• CAS No.: 1228272-03-4
• Molecular Formula: C₁₆H₉N₅O₄S
• Molecular Weight: 367.345
• Mol file: 1228272-03-4.mol

Synonyms:10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine

Chemical Property of 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine

There total 3 articles about 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

10H-dipyrido[3,4-b:3',4'-e][1,4]thiazine (503321-47-9) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine (1228272-03-4)

Guidance literature:

10H-dipyrido[3,4-b:3',4'-e][1,4]thiazine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

2,4-Dinitrofluorobenzene; In N,N-dimethyl-formamide; for 24h;

DOI:10.1002/ardp.200900253

Reference yield:

3-chloro-4-nitropyridine (13194-60-0) → 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine (1228272-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 24 h

With sodium hydride; sodium hydroxide; In N,N-dimethyl-formamide;

DOI:10.1002/ardp.200900253

Reference yield:

3-aminopyridine-4(1H)-thione (38240-23-2) → 10-(2',4'-dinitrophenyl)-2,7-diazaphenothiazine (1228272-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 24 h

With sodium hydride; sodium hydroxide; In N,N-dimethyl-formamide;

DOI:10.1002/ardp.200900253

upstream raw materials:

10H-dipyrido[3,4-b:3',4'-e][1,4]thiazine

2,4-Dinitrofluorobenzene

3-chloro-4-nitropyridine

3-aminopyridine-4(1H)-thione