7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

Base Information

Chemical Name:7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole
CAS No.:107804-69-3
Molecular Formula:C₁₈H₁₄BrNO₄
Molecular Weight:388.217
Hs Code.:

Synonyms:7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

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Chemical Property of 7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

Chemical Property:

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Technology Process of 7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

There total 6 articles about 7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107804-45-5
7,8-dihydro-3-phenylfuro[2,3-g]-1,2-benzisoxazole-7-methanol

: 107804-69-3
7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

Guidance literature:: With bromine; acetic anhydride; In dichloromethane; benzene;

Reference yield:

: 136741-67-8
6-hydroxy-3-phenyl-1,2-benzisoxazole

: 107804-69-3
7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 2.5 h / 50 - 60 °C

2: 44 percent / N,N-dimethylaniline / 1 h / Heating

3: 99 percent / m-chloroperbenzoic acid / CHCl₃ / 5 h / Heating

4: 2) Br₂ / 1) benzene, 5h, reflux 2) CH₂Cl₂, r.t., 10h

With bromine; potassium carbonate; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.1760

Reference yield:

: 136741-51-0
6-Methoxy-3-phenyl-benzo[d]isoxazole

: 107804-69-3
7-acetoxymethyl-5-bromo-7,8-dihydro-3-phenylfuro<2,3-g>-1,2-benzisoxazole

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / pyridine hydrochloride / 7 h / 180 - 190 °C

2: 98 percent / K₂CO₃ / dimethylformamide / 2.5 h / 50 - 60 °C

3: 44 percent / N,N-dimethylaniline / 1 h / Heating

4: 99 percent / m-chloroperbenzoic acid / CHCl₃ / 5 h / Heating

5: 2) Br₂ / 1) benzene, 5h, reflux 2) CH₂Cl₂, r.t., 10h

With bromine; pyridine hydrochloride; potassium carbonate; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.1760