C₃₀H₃₂N₂

Base Information

Chemical Name:C₃₀H₃₂N₂
CAS No.:1332883-47-2
Molecular Formula:C₃₀H₃₂N₂
Molecular Weight:420.597
Hs Code.:

C<sub>30</sub>H<sub>32</sub>N<sub>2</sub>

Synonyms:C₃₀H₃₂N₂

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Chemical Property of C₃₀H₃₂N₂

Chemical Property:

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Technology Process of C₃₀H₃₂N₂

There total 3 articles about C₃₀H₃₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 107-15-3,85404-18-8
ethylenediamine

: 756873-19-5
4-bromo-(3,5-dimethyl)biphenyl

: 1332883-47-2
C₃₀H₃₂N₂

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene; at 100 ℃; for 44h; Inert atmosphere;
DOI:10.1039/c1cc13304g

Reference yield:

: 689260-53-5
2-bromo-5-iodo-1,3-dimethylbenzene

: 1332883-47-2
C₃₀H₃₂N₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; sodium carbonate; triphenylphosphine; phenylboronic acid / water; acetone / 18 h / Reflux; Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 44 h / 100 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; sodium t-butanolate; phenylboronic acid; In water; acetone; toluene;
DOI:10.1039/c1cc13304g

Reference yield:

: 59557-90-3
4-bromo-3,5-dimethylaniline

: 1332883-47-2
C₃₀H₃₂N₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / water / 0.42 h / -10 °C / Inert atmosphere

1.2: 2.33 h / -10 - 0 °C / Inert atmosphere

2.1: palladium diacetate; sodium carbonate; triphenylphosphine; phenylboronic acid / water; acetone / 18 h / Reflux; Inert atmosphere

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 44 h / 100 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; palladium diacetate; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; sodium t-butanolate; sodium nitrite; phenylboronic acid; In water; acetone; toluene;
DOI:10.1039/c1cc13304g