(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

Base Information

Chemical Name:(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate
CAS No.:1093865-39-4
Molecular Formula:C₂₄H₃₈N₂O₄Si
Molecular Weight:446.662
Hs Code.:

Synonyms:(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

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Chemical Property of (S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

Chemical Property:

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Technology Process of (S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

There total 1 articles about (S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 884511-14-2
(S)-2-(trimethylsilyl)ethyl 2-amino-3-cyclohexylpropyl(methyl)carbamate

: 619-21-6
m-formylphenyl benzoic acid

: 1093865-39-4
(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 20h;

Reference yield: 42.0%

: 1093865-39-4
(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

: 36229-42-2
(3-chlorophenyl)magnesium bromide

: 1093865-40-7
2-(trimethylsilyl)ethyl (2S)-2-(3-((3-chlorophenyl)(hydroxy)methyl)benzamido)-3-cyclohexylpropyl(methyl)carbamate

Guidance literature:: (S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate; (3-chlorophenyl)magnesium bromide; In tetrahydrofuran; at 0 ℃; for 7h;

With water; sodium carbonate; In tetrahydrofuran;

Reference yield:

: 1093865-39-4
(S)-2-(trimethylsilyl)ethyl 3-cyclohexyl-2-(3-formylbenzamido)-propyl(methyl)carbamate

: 1093865-41-8
3-((3-chlorophenyl)(2-(2,2,2-trifluoroacetamido)ethoxy)methyl)-N-((S)-1-cyclohexyl-3-(methylamino)propan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 7 h / 0 °C

2: toluene-4-sulfonic acid / 4.5 h / 140 °C

With toluene-4-sulfonic acid; In tetrahydrofuran;