1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

Base Information

Chemical Name:1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose
CAS No.:88152-92-5
Molecular Formula:C₄₇H₄₈O₁₂S
Molecular Weight:836.957
Hs Code.:

Synonyms:1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

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Chemical Property of 1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

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Technology Process of 1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

There total 1 articles about 1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.6%

: 100-39-0
benzyl bromide

: 78101-90-3
1,6-anhydro-4',6'-O-benzylidene-2'-O-tosyl-β-maltose

: 88121-28-2
1,6-anhydro-4-O-(2,3-anhydro-4,6-O-benzylidene-α-D-mannopyranosyl)-2,3-di-O-benzyl-β-D-glucopyranose

: 88152-92-5
1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

Guidance literature:: With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; 1.) 0 deg C, 2 h, 2.) 10 deg C, 40 h;

Reference yield: 90.8%

: 88152-92-5
1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

: 88121-29-3
1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-β-maltose

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; methanol; for 5h; Heating;

Reference yield:

: 88152-92-5
1,6-anhydro-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-2'-O-(p-toluenesulfonyl)-β-maltose

: 88121-30-6
1,6-anhydro-2'-O-acetyl-2,3,3'-tri-O-benzyl-4',6'-O-benzylidene-β-maltose

Guidance literature:: Multi-step reaction with 2 steps

1: 90.8 percent / 8 N KOH / dioxane; methanol / 5 h / Heating

2: 86 percent / pyridine / Ambient temperature

With pyridine; potassium hydroxide; In 1,4-dioxane; methanol;