Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

Base Information

Chemical Name:Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid
CAS No.:141020-13-5
Molecular Formula:C₃₅H₃₀O₁₀S
Molecular Weight:642.683
Hs Code.:

Synonyms:Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

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Technology Process of Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

There total 1 articles about Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3601-36-3,6344-46-3
methyl 2,3,6-tri-O-benzoyl-α-D-galactopyranoside

: 1005-56-7
phenylcarbonochloridothioate

: 141020-13-5
Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

Guidance literature:: With pyridine; In dichloromethane; for 48h; Ambient temperature;

Reference yield: 94.0%

: 141020-13-5
Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

: 19488-41-6
Methyl-2,3,6-tri-O-benzoyl-4-desoxy-α-D-xylo-hexopyranosid

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; for 4h; Heating;

Reference yield:

: 141020-13-5
Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

: C₄₂H₄₃NO₁₃

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / Bu3SnH, α,α'-azoisobutyronitrile / toluene / 4 h / Heating

2: 94 percent / iodotrimethylsilane / toluene / 3 h / Ambient temperature

3: 1.) Hg(CN)2, molecular sieves 4 Angstroem / 1.) dichloromethane, 1 h, 2.) 10 deg C, 5 h

4: 60 percent aq. acetic acid / 3 h / 40 °C

With trimethylsilyl iodide; 4 A molecular sieve; azobisisobutyronitrile; tri-n-butyl-tin hydride; mercury(II) cyanide; acetic acid; In toluene;