sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

Base Information

Chemical Name:sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate
CAS No.:1254160-17-2
Molecular Formula:C₁₆H₂₁ClN₅O₇S*Na
Molecular Weight:485.881
Hs Code.:

Synonyms:sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

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Chemical Property of sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

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Technology Process of sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

There total 7 articles about sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338586-49-4
2-chloro-2',3'-isopropylidene-N⁶-cyclohexyladenosine

: 1254160-17-2
sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfur trioxide / N,N-dimethyl-formamide / 20 °C

1.2: pH 7

2.1: trifluoroacetic acid; water / 0.5 h

With sulfur trioxide; water; trifluoroacetic acid; In N,N-dimethyl-formamide;

Reference yield:

: C₁₉H₂₅ClN₅O₇S^(1-)*Na⁽¹⁺⁾

: 1254160-17-2
sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

Guidance literature:: With water; trifluoroacetic acid; for 0.5h;

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 1254160-17-2
sodium ((2R,3S,4R,5R)-5-(2-chloro-6-(cyclohexylamino)-9H-purin-9-yl)-3,4-dihydroxytetrahydrofuran-2-yl)methyl sulfate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 6 h / Reflux

2.1: (1S)-10-camphorsulfonic acid / acetone / 4 h / 20 °C

3.1: sulfur trioxide / N,N-dimethyl-formamide / 20 °C

3.2: pH 7

4.1: trifluoroacetic acid; water / 0.5 h

With (1S)-10-camphorsulfonic acid; sulfur trioxide; water; trifluoroacetic acid; In ethanol; N,N-dimethyl-formamide; acetone;