C₂₄H₂₈ClNO₆

Base Information

Chemical Name:C₂₄H₂₈ClNO₆
CAS No.:1258864-05-9
Molecular Formula:C₂₄H₂₈ClNO₆
Molecular Weight:461.942
Hs Code.:

C<sub>24</sub>H<sub>28</sub>ClNO<sub>6</sub>

Synonyms:C₂₄H₂₈ClNO₆

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Chemical Property of C₂₄H₂₈ClNO₆

Chemical Property:

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Technology Process of C₂₄H₂₈ClNO₆

There total 13 articles about C₂₄H₂₈ClNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 5061-21-2
α-bromo-γ-butyrolactone

: 1258864-04-8
C₂₀H₂₂ClNO₄

: 1258864-05-9
C₂₄H₂₈ClNO₆

: 1258864-09-3
C₂₄H₂₈ClNO₆

Guidance literature:: With Wilkinson's catalyst; diethylzinc; In tetrahydrofuran; at -20 ℃; for 3h;
DOI:10.3987/COM-10-12042

Reference yield:

: C₉H₁₇NO₂

: 1258864-05-9
C₂₄H₂₈ClNO₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

3.1: methanol / diethyl ether / 0 °C

4.1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

5.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

5.2: 0.25 h

6.1: sodium tetrahydroborate / methanol / 2 h / -40 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / Reflux

8.1: diisobutylaluminium hydride / tetrahydrofuran / 9 h / -5 °C

9.1: dmap; triethylamine / dichloromethane / 3 h / Reflux

10.1: dimethylaluminum chloride / hexane; dichloromethane / 0.5 h / 0 - 20 °C

11.1: 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 12 h / 20 °C

12.1: Wilkinson's catalyst; diethylzinc / tetrahydrofuran / 3 h / -20 °C

With methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium tetrahydroborate; Wilkinson's catalyst; 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene; diethylzinc; dimethylaluminum chloride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; 5.1: Claisen condensation / 5.2: Claisen condensation / 12.1: Reformatsky reaction;
DOI:10.3987/COM-10-12042

Reference yield:

: 1258863-99-8
C₁₆H₂₀ClNO₃

: 1258864-05-9
C₂₄H₂₈ClNO₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / water; acetonitrile / 15 h / 0 °C

2.1: methanol / diethyl ether / 0 °C

3.1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

4.2: 0.25 h

5.1: sodium tetrahydroborate / methanol / 2 h / -40 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / Reflux

7.1: diisobutylaluminium hydride / tetrahydrofuran / 9 h / -5 °C

8.1: dmap; triethylamine / dichloromethane / 3 h / Reflux

9.1: dimethylaluminum chloride / hexane; dichloromethane / 0.5 h / 0 - 20 °C

10.1: 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 12 h / 20 °C

11.1: Wilkinson's catalyst; diethylzinc / tetrahydrofuran / 3 h / -20 °C

With methanol; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium tetrahydroborate; Wilkinson's catalyst; 1-methyl-2-azaadamantane-N-oxyl; [bis(acetoxy)iodo]benzene; diethylzinc; dimethylaluminum chloride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; 4.1: Claisen condensation / 4.2: Claisen condensation / 11.1: Reformatsky reaction;
DOI:10.3987/COM-10-12042