2,2'-Diacetoxydiphenylacetylene

Base Information

Chemical Name:2,2'-Diacetoxydiphenylacetylene
CAS No.:328945-91-1
Molecular Formula:C₁₈H₁₄O₄
Molecular Weight:294.307
Hs Code.:

Synonyms:2,2'-Diacetoxydiphenylacetylene

Suppliers and Price of 2,2'-Diacetoxydiphenylacetylene

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Chemical Property of 2,2'-Diacetoxydiphenylacetylene

Chemical Property:

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Technology Process of 2,2'-Diacetoxydiphenylacetylene

There total 2 articles about 2,2'-Diacetoxydiphenylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32865-61-5
2-iodophenyl acetate

: 74-86-2,25067-58-7
acetylene

: 328945-91-1
2,2'-Diacetoxydiphenylacetylene

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 60 ℃; for 16h;
DOI:10.1039/b006623k

Reference yield:

: 533-58-4
2-Iodophenol

: 328945-91-1
2,2'-Diacetoxydiphenylacetylene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 20 °C

2: 0.45 g / CuI; Et₃N / PdCl₂(PPh₃)2 / dimethylformamide / 16 h / 60 °C

With pyridine; copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide;
DOI:10.1039/b006623k