6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

Base Information

Chemical Name:6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside
CAS No.:164112-40-7
Molecular Formula:C₃₆H₄₂O₉
Molecular Weight:618.724
Hs Code.:

Synonyms:6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

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Chemical Property of 6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

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Technology Process of 6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

There total 9 articles about 6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 98-88-4
benzoyl chloride

: 164112-38-3
6-(phenylmethoxy)-1-hexyl 3,4-O-isopropylidene-β-D-galactopyranoside

: 164112-40-7
6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: With pyridine; dmap; for 24h; Ambient temperature;
DOI:10.1021/ja00104a011

Reference yield:

: 5299-60-5
6-hydroxy-hexanoic acid ethyl ester

: 164112-40-7
6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 42.06 g / TfOH / CH₂Cl₂ / 18 h / 0 °C

2: LiAlH₄ / tetrahydrofuran / 6 h / Ambient temperature

3: BF₃*Et₂O / CH₂Cl₂ / 1.5 h / 0 °C

4: NaOMe, MeOH / 6 h / Ambient temperature

5: p-TsOH / 18 h / Ambient temperature

6: 86 percent / DMAP, pyridine / 24 h / Ambient temperature

With pyridine; methanol; dmap; lithium aluminium tetrahydride; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00104a011

Reference yield:

: 56175-38-3
ethyl 6-(phenylmethoxy)hexanoate

: 164112-40-7
6-(phenylmethoxy)-1-hexyl 2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: LiAlH₄ / tetrahydrofuran / 6 h / Ambient temperature

2: BF₃*Et₂O / CH₂Cl₂ / 1.5 h / 0 °C

3: NaOMe, MeOH / 6 h / Ambient temperature

4: p-TsOH / 18 h / Ambient temperature

5: 86 percent / DMAP, pyridine / 24 h / Ambient temperature

With pyridine; methanol; dmap; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00104a011