3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

Base Information

Chemical Name:3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide
CAS No.:1609152-91-1
Molecular Formula:C₂₄H₂₂Cl₂N₂O₅
Molecular Weight:489.355
Hs Code.:

Synonyms:3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

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Technology Process of 3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

There total 5 articles about 3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.8%

: 1185160-66-0
3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

: 99-93-4
4-Hydroxyacetophenone

: 1609152-91-1
3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

Guidance literature:: 3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine; With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

4-Hydroxyacetophenone; In N,N-dimethyl-formamide; at 75 ℃; for 10h;
DOI:10.3184/174751913X13782291519608

Reference yield:

: 621-59-0
isovanillin

: 1609152-91-1
3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 10 h / 75 °C

2.1: aminosulfonic acid; acetic acid; sodium chlorite / water / 1 h / 0 - 5 °C / Cooling with ice

3.1: thionyl chloride / 2 h / Reflux

4.1: sodium hydride / tetrahydrofuran / 5 h / 15 - 25 °C

5.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 10 h / 75 °C

With sodium chlorite; thionyl chloride; aminosulfonic acid; sodium hydride; potassium carbonate; acetic acid; potassium iodide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.3184/174751913X13782291519608

Reference yield:

: 1609152-85-3
C₁₁H₁₂Cl₂O₃

: 1609152-91-1
3-(3-(4-Acetylphenoxy)propoxy)-N-(3,5-dichloropyridin-4-yl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 5 h / 15 - 25 °C

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 10 h / 75 °C

With sodium hydride; potassium carbonate; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3184/174751913X13782291519608