(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

Base Information

Chemical Name:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate
CAS No.:1559057-62-3
Molecular Formula:C₅₁H₅₀F₂O₇
Molecular Weight:812.951
Hs Code.:

(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

Synonyms:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

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Chemical Property of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

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Technology Process of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

There total 4 articles about (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1559057-48-5
(1S,2R,3R,4R)-3-[(1E)-3-oxo-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

: 1559057-62-3
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

Guidance literature:: With DeoxoFluor; In tetrahydrofuran; at 5 - 37 ℃; for 24h;

Reference yield:

: 1559057-77-0,130209-78-8
C₂₅H₃₆O₆

: 1559057-62-3
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; 1,4-dioxane / 11 h / 25 - 40 °C

2: pyridine / dichloromethane / 2 h / 5 - 25 °C

3: DeoxoFluor / tetrahydrofuran / 24 h / 5 - 37 °C

With pyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1559057-74-7
(Z)-isopropyl 7-((1R,5S,6R,7R)-7-((E)-3-hydroxy-4-phenoxybut-1-en-1-yl)-3-phenyl-2,4-dioxa-3-borabicyclo[3.2.1]octan-6-yl)hept-5-enoate

: 1559057-62-3
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]-4-[(4-phenylphenyl)carbonyloxy]cyclopentyl 4-phenylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: PCC on alumina / dichloromethane / 3 h / 25 °C

2: pyridine / dichloromethane / 2 h / 5 - 25 °C

3: DeoxoFluor / tetrahydrofuran / 24 h / 5 - 37 °C

With pyridine; PCC on alumina; In tetrahydrofuran; dichloromethane;