(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

Base Information

Chemical Name:(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide
CAS No.:136025-85-9
Molecular Formula:C₁₈H₂₂N₂O₅
Molecular Weight:346.383
Hs Code.:

Synonyms:(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

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Chemical Property of (S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

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Technology Process of (S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

There total 7 articles about (S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 136025-84-8,136025-89-3
(S)-(+)-6-sec-butyl-3-(α-hydroxy-p-methoxymethoxybenzyl)-2-methoxypyrazine 4-oxide

: 136025-85-9
(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

Guidance literature:: With Collins oxidation agent; In dichloromethane; for 3h; Ambient temperature;
DOI:10.3987/COM-91-5682

Reference yield:

: 136025-81-5
(S)-(+)-6-sec-butyl-2-methoxy-3-methyl-3-methylpyrazine

: 136025-85-9
(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 43 percent / benzeneselenic anhydride (BSA) / chlorobenzene / 6 h

2: 1.) Mg, I₂ / 1.) Et₂O, THF, reflux, 30 min, 2.) Et₂O, THF, RT, 6 h

3: 98 percent / permaleic acid / CHCl₃

4: 99 percent / Collins reagent / CH₂Cl₂ / 3 h / Ambient temperature

With monopermaleic acid; Collins oxidation agent; benzeneseleninic anhydride; iodine; magnesium; In dichloromethane; chloroform; chlorobenzene;
DOI:10.3987/COM-91-5682

Reference yield:

: 136025-82-6
(S)-(+)-6-sec-butyl-3-formyl-2-methoxypyrazine

: 136025-85-9
(S)-(+)-sec-butyl-2-methoxy-3-(p-methoxymethoxybenzyl)-pyrazine 4-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, I₂ / 1.) Et₂O, THF, reflux, 30 min, 2.) Et₂O, THF, RT, 6 h

2: 98 percent / permaleic acid / CHCl₃

3: 99 percent / Collins reagent / CH₂Cl₂ / 3 h / Ambient temperature

With monopermaleic acid; Collins oxidation agent; iodine; magnesium; In dichloromethane; chloroform;
DOI:10.3987/COM-91-5682