methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside
CAS No.:131326-62-0
Molecular Formula:C₂₂H₂₇N₃O₆
Molecular Weight:429.473
Hs Code.:

Synonyms:methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

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Chemical Property of methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

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Technology Process of methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

There total 3 articles about methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2746-25-0
p-Methoxybenzyl bromide

: 258286-29-2
methyl 2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside

: 131326-62-0
methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

Guidance literature:: methyl 2-azido-6-O-benzyl-2-desoxy-α-D-galactopyranoside; With di(n-butyl)tin oxide; In acetonitrile; at 80 ℃; for 14h;

p-Methoxybenzyl bromide; With tetra-(n-butyl)ammonium iodide; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1016/s0040-4020(99)00869-8

Reference yield:

: 128716-56-3
2-azido-6-O-benzyl-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranosyl nitrate

: 131326-62-0
methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 64 percent / methanol / 4 h / 20 °C

2.1: 95 percent / de l'acide acetique 80 percent / 0.17 h / 80 °C

3.1: nBu₂SnO / acetonitrile / 14 h / 80 °C

3.2: 90 percent / NBu₄I / acetonitrile / 48 h / 20 °C

With de l'acide acetique; di(n-butyl)tin oxide; In methanol; acetonitrile; 1.1: Substitution / 2.1: Hydrolysis / 3.1: Substitution / 3.2: Substitution;
DOI:10.1016/s0040-4020(99)00869-8

Reference yield:

: 258286-28-1
methyl 2-azido-6-O-benzyl-2-desoxy-3,4-O-isopropylidene-α-D-galactopyranoside

: 131326-62-0
methyl 2-azido-6-O-benzyl-2-desoxy-3-O-p-methoxybenzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / de l'acide acetique 80 percent / 0.17 h / 80 °C

2.1: nBu₂SnO / acetonitrile / 14 h / 80 °C

2.2: 90 percent / NBu₄I / acetonitrile / 48 h / 20 °C

With de l'acide acetique; di(n-butyl)tin oxide; In acetonitrile; 1.1: Hydrolysis / 2.1: Substitution / 2.2: Substitution;
DOI:10.1016/s0040-4020(99)00869-8