5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

Base Information

Chemical Name:5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)
CAS No.:1539328-18-1
Molecular Formula:C₄₂H₃₈N₈NiO₄
Molecular Weight:777.505
Hs Code.:

Synonyms:5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

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Chemical Property of 5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

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Technology Process of 5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

There total 5 articles about 5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 876863-25-1
5-(tert-butoxycarbonylazo)-10,20-diphenylporphyrinatonickel(II)

: 1539328-18-1
5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

Guidance literature:: With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; for 336h;
DOI:10.1016/j.tet.2013.11.006

Reference yield: 19.0%

: 193265-35-9
[10-bromo-5,15-diphenylporphyrinato]-magnesium(II)

: 870-46-2
t-butoxycarbonylhydrazine

: 866916-96-3
5-[(tert-butoxycarbonyl)hydrazo]-10,20-diphenylporphyrinatonickel(II)

: 1539328-18-1
5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 68 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2013.11.006

Reference yield:

: 193265-35-9
[10-bromo-5,15-diphenylporphyrinato]-magnesium(II)

: 870-46-2
t-butoxycarbonylhydrazine

: 876863-25-1
5-(tert-butoxycarbonylazo)-10,20-diphenylporphyrinatonickel(II)

: 1539328-18-1
5,15-[N,N'-bis(tert-butoxycarbonylamino)]diimino-10,20-diphenylporphodimethenatonickel(II)

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 68 ℃; for 27h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2013.11.006