C₃₂H₁₉NO

Base Information

Chemical Name:C₃₂H₁₉NO
CAS No.:1427675-64-6
Molecular Formula:C₃₂H₁₉NO
Molecular Weight:433.509
Hs Code.:

Synonyms:C₃₂H₁₉NO

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Chemical Property of C₃₂H₁₉NO

Chemical Property:

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Technology Process of C₃₂H₁₉NO

There total 11 articles about C₃₂H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1427675-62-4
(PM)-1-aza[6]helicen-15-yl trifluoromethanesulfonate

: 40138-16-7
2-formylbenzene boronic acid

: 1427675-64-6
C₃₂H₁₉NO

Guidance literature:: With palladium diacetate; sodium carbonate; triphenylphosphine; In 1,4-dioxane; water; at 100 ℃;
DOI:10.1021/ol400493x

Reference yield:

: 1427675-52-2
1-bromo-2-(2’-trimethylsilyl)ethynylnaphthalene

: 1427675-64-6
C₃₂H₁₉NO

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

3.1: platinum(IV) chloride / 1,2-dichloro-ethane / 16 h / 120 °C / Inert atmosphere; Sealed tube

4.1: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane; n-heptane / 0.01 h / -78 - 20 °C

5.1: pyridine / dichloromethane / 20 °C

6.1: palladium diacetate; triphenylphosphine; sodium carbonate / 1,4-dioxane; water / 100 °C

With pyridine; n-butyllithium; tetrabutyl ammonium fluoride; palladium diacetate; boron trichloride; platinum(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium carbonate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; hexane; n-heptane; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/ol400493x

Reference yield:

: 1427675-54-4
(RS)-10-(7’-methoxy-2’-((trimethylsilyl)ethynyl)naphthalen-1’-yl)benzo[h]quinoline

: 1427675-64-6
C₃₂H₁₉NO

Guidance literature:: Multi-step reaction with 5 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2: platinum(IV) chloride / 1,2-dichloro-ethane / 16 h / 120 °C / Inert atmosphere; Sealed tube

3: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane; n-heptane / 0.01 h / -78 - 20 °C

4: pyridine / dichloromethane / 20 °C

5: palladium diacetate; triphenylphosphine; sodium carbonate / 1,4-dioxane; water / 100 °C

With pyridine; tetrabutyl ammonium fluoride; palladium diacetate; boron trichloride; platinum(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium carbonate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; n-heptane; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/ol400493x