O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

Base Information

Chemical Name:O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate
CAS No.:154592-65-1
Molecular Formula:C₁₉H₂₈ClNOSe
Molecular Weight:400.85
Hs Code.:

Synonyms:O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

Chemical Property:

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Technology Process of O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

There total 4 articles about O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1724-39-6
cyclododecanol

: 14223-48-4
p-chlorophenyl isoselenocyanate

: 154592-65-1
O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

Guidance literature:: With potassium hydride; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80783-3

Reference yield:

: 2617-79-0
N-(4-chlorophenyl)formamide

: 154592-65-1
O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Et₃N, Se(powder), phosgene / toluene / 0 - 110 °C

2: 88 percent / potassium hydride / tetrahydrofuran / 4 h / Ambient temperature

With phosgene; selenium; potassium hydride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)80783-3

Reference yield:

: 106-47-8
4-chloro-aniline

: 154592-65-1
O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 12 h / Heating

2: 65 percent / Et₃N, Se(powder), phosgene / toluene / 0 - 110 °C

3: 88 percent / potassium hydride / tetrahydrofuran / 4 h / Ambient temperature

With phosgene; selenium; potassium hydride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)80783-3