ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

Base Information

Chemical Name:ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate
CAS No.:53295-33-3
Molecular Formula:C₃₂H₃₀N₂O₂
Molecular Weight:474.602
Hs Code.:

Synonyms:ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

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Chemical Property of ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

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Technology Process of ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

There total 4 articles about ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 141-97-9
ethyl acetoacetate

: 100-52-7
benzaldehyde

: 62-53-3
aniline

: 53295-33-3
ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With bismuth(III) immobilized on triazine dendrimer stabilized magnetic nanoparticle; In ethanol; at 20 ℃; for 1h; Solvent; Reagent/catalyst; Catalytic behavior;
DOI:10.1021/acscombsci.6b00180

Reference yield: 20.0%

: 15206-97-0
Ethyl α-acetyl-β-anilino-β-phenylpropionate

: 100-52-7
benzaldehyde

: 62-53-3
aniline

: 53295-33-3
ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With malonic acid; In ethanol; for 1h; Heating;
DOI:10.1007/BF00552778

Reference yield:

: 141-97-9
ethyl acetoacetate

: 53295-33-3
ethyl 2,6-bis-phenyl-1-phenyl-4-phenylamino-1,2,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 20 percent / malonic acid / ethanol / 1 h / Heating

With malonic acid; In ethanol;
DOI:10.1007/BF00552778