(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

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Chemical Name:(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine
CAS No.:1211510-07-4
Molecular Formula:C₂₈H₁₉N₇
Molecular Weight:453.506
Hs Code.:

Synonyms:(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

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Chemical Property of (5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

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Technology Process of (5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

There total 1 articles about (5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 504-29-0
2-aminopyridine

: 52197-23-6
5,6-diphenyl-pyrazine-2,3-dicarbonitrile

: 1211510-07-4
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

Guidance literature:: With calcium chloride; In butan-1-ol; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/ic902019s

Reference yield: 65.0%

: 36389-82-9,24940-43-0,36389-81-8
dichlorobis(tetrahydrothiophene)platinum(II)

: 1211510-07-4
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

: 1211509-94-2
chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

Guidance literature:: With Et₃N; In methanol; under Ar; mixt. of Pt complex, ligand and Et3N in MeOH refluxed for 12 h; cooled to room temp.; filtered; ppt. washed with H2O, EtOH and Et2O; dried in vac.; recrystd. from CH2Cl2-n-hexane; elem. anal.;
DOI:10.1021/ic902019s

Reference yield:

: 1211510-07-4
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

: 1211510-06-3
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))(4-tert-butylphenylethynyl)platinum(II)

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / methanol

2: Et₃N / copper(l) iodide / dichloromethane

With Et₃N; copper(l) iodide; In methanol; dichloromethane;
DOI:10.1021/ic902019s