chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

Base Information

Chemical Name:chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)
CAS No.:1211509-94-2
Molecular Formula:C₂₈H₁₈ClN₇Pt
Molecular Weight:683.031
Hs Code.:

Synonyms:chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

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Chemical Property of chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

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Technology Process of chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

There total 1 articles about chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 36389-82-9,24940-43-0,36389-81-8
dichlorobis(tetrahydrothiophene)platinum(II)

: 1211510-07-4
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]-pyrazin-7-ylidene)pyridin-2-amine

: 1211509-94-2
chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

Guidance literature:: With Et₃N; In methanol; under Ar; mixt. of Pt complex, ligand and Et3N in MeOH refluxed for 12 h; cooled to room temp.; filtered; ppt. washed with H2O, EtOH and Et2O; dried in vac.; recrystd. from CH2Cl2-n-hexane; elem. anal.;
DOI:10.1021/ic902019s

Reference yield: 75.0%

: 14323-41-2
potassium tetracyanonickelate(II) dihydrate

: 1211509-94-2
chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

: C₂₉H₁₈N₈Pt

Guidance literature:: In methanol; for 24h; Reflux;
DOI:10.1002/ejic.201300622

Reference yield: 68.0%

: 1211509-94-2
chloro(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))platinum(II)

: 772-38-3
4-tert-Butylphenylacetylene

: 1211510-06-3
(5,6-dihydro-2,3-diphenyl-5-(pyridin-2-ylimino)pyrrolo[3,4-b]pyrazin-7-ylidene(-1H))(4-tert-butylphenylethynyl)platinum(II)

Guidance literature:: With Et₃N; copper(l) iodide; In dichloromethane; under Ar; mixt. of Pt complex, t-BuC6H4CCH, CuI (catalytic amt.) and Et3N in CH2Cl2 refluxed for 12 h; cooled to room temp.; filtered; filtrate evapd. to dryness under reduced pressure; purified bycolumn chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/ic902019s