2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

Base Information

Chemical Name:2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid
CAS No.:1414948-04-1
Molecular Formula:C₂₇H₂₅BrO₈
Molecular Weight:557.395
Hs Code.:

Synonyms:2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

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Chemical Property of 2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

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Technology Process of 2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

There total 3 articles about 2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 127987-16-0
(2,3,7,8,12,13)-hexamethoxy-5H-tribenzo[a,d,g]cyclononene-5,10(15H)-dione

: 1414948-04-1
2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In 1,2-dichloro-ethane; at 70 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo302139w

Reference yield: 18.4%

: 64-17-5
ethanol

: 127987-16-0
(2,3,7,8,12,13)-hexamethoxy-5H-tribenzo[a,d,g]cyclononene-5,10(15H)-dione

: 1414948-04-1
2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

: 1414948-06-3
2-ethyl (10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoate

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In chloroform; at 70 ℃; for 5.5h; Inert atmosphere;
DOI:10.1021/jo302139w

Reference yield:

: 1180-60-5
cyclotriveratrylene

: 1414948-04-1
2-(10-bromo-2,3,6,7-tetramethoxyanthracen-9-yl)-4,5-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium permanganate; manganese(IV) oxide; pyridine / 18 h / Reflux; Inert atmosphere

2: N-Bromosuccinimide; dibenzoyl peroxide / 1,2-dichloro-ethane / 2 h / 70 °C / Inert atmosphere

With pyridine; manganese(IV) oxide; potassium permanganate; N-Bromosuccinimide; dibenzoyl peroxide; In 1,2-dichloro-ethane;
DOI:10.1021/jo302139w