(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

Base Information

Chemical Name:(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol
CAS No.:1227674-37-4
Molecular Formula:C₂₁H₂₄Br₂I₂O
Molecular Weight:706.038
Hs Code.:

Synonyms:(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

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Chemical Property of (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

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Technology Process of (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

There total 3 articles about (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1227674-36-3
4-tert-butyl-2,6-diiodobenzaldehyde

: 172368-00-2
1,3-dibromo-5-(tert-butyl)-2-iodobenzene

: 1227674-37-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

Guidance literature:: 1,3-dibromo-5-(tert-butyl)-2-iodobenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 5h;

4-tert-butyl-2,6-diiodobenzaldehyde; In diethyl ether; hexane; at -78 - 20 ℃;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-34-1
4-tert-butyl-2,6-diiodobenzyl acetate

: 1227674-37-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / methanol / 3 h / 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

3.2: -78 - 20 °C

With n-butyllithium; potassium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1002/poc.1651

Reference yield:

: 405313-64-6
5-(tert-butyl)-1,3-diiodo-2-methylbenzene

: 1227674-37-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium permanganate; sulfuric acid; acetic acid / 40 °C

2.1: potassium carbonate / methanol / 3 h / 20 °C

3.1: pyridinium chlorochromate / dichloromethane / 20 °C

4.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

4.2: -78 - 20 °C

With potassium permanganate; n-butyllithium; sulfuric acid; potassium carbonate; acetic acid; pyridinium chlorochromate; In methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1002/poc.1651