(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

Base Information

Chemical Name:(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane
CAS No.:1227674-38-5
Molecular Formula:C₂₁H₂₃Br₂ClI₂
Molecular Weight:724.484
Hs Code.:

Synonyms:(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

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Chemical Property of (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

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Technology Process of (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

There total 6 articles about (2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1227674-37-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methanol

: 1227674-38-5
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

Guidance literature:: With thionyl chloride; at 20 ℃;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-36-3
4-tert-butyl-2,6-diiodobenzaldehyde

: 1227674-38-5
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

1.2: -78 - 20 °C

2.1: thionyl chloride / 20 °C

With n-butyllithium; thionyl chloride; In diethyl ether; hexane;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-34-1
4-tert-butyl-2,6-diiodobenzyl acetate

: 1227674-38-5
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / methanol / 3 h / 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

3.2: -78 - 20 °C

4.1: thionyl chloride / 20 °C

With n-butyllithium; thionyl chloride; potassium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1002/poc.1651