ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

Base Information

Chemical Name:ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate
CAS No.:183430-93-5
Molecular Formula:C₂₀H₃₀N₄O₆
Molecular Weight:422.481
Hs Code.:

Synonyms:ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

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Chemical Property of ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

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Technology Process of ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

There total 1 articles about ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1949-51-5
3,5-diaminobenzoic acid ethyl ester

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: 183430-93-5
ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; 1.) 0 deg C, 0.5 h, 2.) RT, 24 h;
DOI:10.1021/jm970479e

Reference yield:

: 183430-93-5
ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

: 3-Amino-5-guanidino-benzoic acid ethyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; Ambient temperature;
DOI:10.1021/jm970479e

Reference yield:

: 183430-93-5
ethyl 3-amino-5-({[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}amino)benzoate

: Sodium; 3-amino-5-guanidino-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / Ambient temperature

2: 3 N aq. NaOH / 0.75 h / Ambient temperature

With sodium hydroxide; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm970479e