Technology Process of C6H4F6OS
There total 3 articles about C6H4F6OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C6H3BrF6S;
With
tert.-butyl lithium;
In
diethyl ether; pentane;
at -70 ℃;
for 0.5h;
With
Trimethyl borate;
In
diethyl ether; pentane;
at -70 ℃;
for 0.5h;
With
sulfuric acid; dihydrogen peroxide; acetic acid;
In
diethyl ether; water; pentane;
at -20 - 35 ℃;
for 2h;
DOI:10.1002/ejoc.200500125
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: H2; Raney Ni / tetrahydrofuran / 20 °C / 750.06 Torr
2.1: HBr; NaNO2 / H2O / 0.5 h / 0 - 2 °C
2.2: CuBr; HBr / H2O / 1 h / 85 °C
3.1: t-BuLi / diethyl ether; pentane / 0.5 h / -70 °C
3.2: B(OMe)3 / diethyl ether; pentane / 0.5 h / -70 °C
3.3: 81 percent / AcOH; H2SO4; H2O2 / diethyl ether; pentane; H2O / 2 h / -20 - 35 °C
With
hydrogen bromide; hydrogen; tert.-butyl lithium; nickel; sodium nitrite;
In
tetrahydrofuran; diethyl ether; water; pentane;
DOI:10.1002/ejoc.200500125
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: HBr; NaNO2 / H2O / 0.5 h / 0 - 2 °C
1.2: CuBr; HBr / H2O / 1 h / 85 °C
2.1: t-BuLi / diethyl ether; pentane / 0.5 h / -70 °C
2.2: B(OMe)3 / diethyl ether; pentane / 0.5 h / -70 °C
2.3: 81 percent / AcOH; H2SO4; H2O2 / diethyl ether; pentane; H2O / 2 h / -20 - 35 °C
With
hydrogen bromide; tert.-butyl lithium; sodium nitrite;
In
diethyl ether; water; pentane;
DOI:10.1002/ejoc.200500125
