4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline

Base Information

• Chemical Name: 4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline
• CAS No.: 23651-51-6
• Molecular Formula: C₂₅H₂₄N₈O₂
• Molecular Weight: 468.518

Synonyms:4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline

Chemical Property of 4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline

Chemical Property:

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Technology Process of 4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline

There total 4 articles about 4-[5-(4-methyl-piperazin-1-yl)-1⁽³⁾H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C27H26N8O3 (1419845-96-7) → 4-[5-(4-methyl-piperazin-1-yl)-1(3)H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline (23651-51-6)

Guidance literature:

With sodium hydroxide; In methanol; water; at 70 ℃; for 4h;

Reference yield:

2-amino-4-<5'-(4''-methylpiperazin-1''-yl)benzimidazol-2'-yl>aniline (23491-49-8) → 4-[5-(4-methyl-piperazin-1-yl)-1(3)H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline (23651-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 1 h / 90 °C

1.2: 23 h / 90 °C

2.1: sodium hydroxide / water; methanol / 4 h / 70 °C

With sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

4-acetamido-3-nitrobenzaldehyde (51818-98-5) → 4-[5-(4-methyl-piperazin-1-yl)-1(3)H,1'(3')H-[2,5']bibenzoimidazolyl-2'-yl]-2-nitro-aniline (23651-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 1 h / 90 °C

1.2: 23 h / 90 °C

2.1: sodium hydroxide / water; methanol / 4 h / 70 °C

With sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;

upstream raw materials:

4-acetamido-3-nitrobenzaldehyde

2-amino-4-<5'-(4''-methylpiperazin-1''-yl)benzimidazol-2'-yl>aniline

C₂₇H₂₆N₈O₃

Downstream raw materials:

C₂₅H₂₆N₈

C₃₄H₃₀N₈O₂

C₃₃H₂₈N₈O₂

C₃₉H₂₇F₅N₈O₂

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