diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

Base Information

Chemical Name:diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate
CAS No.:216007-25-9
Molecular Formula:C₂₈H₂₆ClN₃O₅S₃
Molecular Weight:616.183
Hs Code.:

Synonyms:diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

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Chemical Property of diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

Chemical Property:

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Technology Process of diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

There total 3 articles about diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52867-26-2
4-chloro-N-sulfinyl-benzenesulfonamide

: 216007-25-9
diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / pyridine / benzene / 3 h / Ambient temperature

2: 2.) Proton Sponge / 1.) CH₂Cl₂, room temperature, 2.) CHCl₃, room temperature

With pyridine; Proton Sponge; In benzene;
DOI:10.1021/jo970737f

Reference yield:

: 98-64-6
4-Chlorobenzenesulfonamide

: 216007-25-9
diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: 96.6 percent / SOCl₂ / 20 h / Heating

2: 94 percent / pyridine / benzene / 3 h / Ambient temperature

3: 2.) Proton Sponge / 1.) CH₂Cl₂, room temperature, 2.) CHCl₃, room temperature

With pyridine; thionyl chloride; Proton Sponge; In benzene;
DOI:10.1021/jo970737f

Reference yield:

: 851-07-0
N,N'-bis-(4-chloro-benzenesulfonyl)-sulfur diimide

: 47547-28-4,78184-79-9
6-aminopenicillanic acid diphenylmethyl ester

: 74-88-4
methyl iodide

: 216007-25-9
diphenylmethyl N-methyl-N-(p-chlorophenylsulfonyl)-S-aminosulfeniminopenicillanate

Guidance literature:: With Proton Sponge; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 2.) CHCl₃, room temperature;
DOI:10.1021/jo970737f