(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

Base Information

Chemical Name:(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester
CAS No.:92598-86-2
Molecular Formula:C₁₉H₂₆N₂O₃
Molecular Weight:330.427
Hs Code.:

Synonyms:(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

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Technology Process of (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

There total 1 articles about (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54-71-7
pilocarpine hydrochloride

: 92598-86-2
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / H₂O / 1 h / 0 - 4 °C

2: 22 percent / dimethylformamide / Ambient temperature

With sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600750109

Reference yield:

: 92598-86-2
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

: 92-13-7
pilocarpine

Guidance literature:: With phosphate buffer; at 37 ℃; Rate constant; pH 7.40;
DOI:10.1002/jps.2600750109

Reference yield:

: 98-88-4
benzoyl chloride

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 92598-86-2
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid phenethyl ester

: Benzoic acid (2R,3S)-2-(3-methyl-3H-imidazol-4-ylmethyl)-3-phenethyloxycarbonyl-pentyl ester; compound with (E)-but-2-enedioic acid

Guidance literature:: With sodium hydrogencarbonate; potassium carbonate; Yield given. Multistep reaction; 1.) toluene, RT, 3 h, 2.) ether, 2-propanol;
DOI:10.1002/jps.2600750811