N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

Base Information

Chemical Name:N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide
CAS No.:112777-44-3
Molecular Formula:C₁₉H₂₀F₃N₃O₄
Molecular Weight:411.381
Hs Code.:

Synonyms:N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

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Chemical Property of N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

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Technology Process of N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

There total 5 articles about N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20265-38-7
3-amino-2-methoxypyridine

: 112777-44-3
N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

Guidance literature:: Multi-step reaction with 5 steps

1: 17.8 g / MgSO₄ / benzene / 1) 2 h reflux 2) stirring at room teperature overnight

2: 41 percent / NaBH₄ / ethanol / 16 h / Heating

3: 71 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

4: tetrahydrofuran / 18 h / Ambient temperature

5: 42 percent / tetrahydrofuran / 4 h

With sodium tetrahydroborate; sodium hydride; magnesium sulfate; In tetrahydrofuran; ethanol; benzene;
DOI:10.1002/jhet.5570240403

Reference yield:

: 20265-35-4
2-methoxy-3-nitropyridine

: 112777-44-3
N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / sulfided platinum / ethanol / 8 h / 150 °C / 51714.8 Torr

2: tetrahydrofuran / 18 h / Ambient temperature

3: 42 percent / tetrahydrofuran / 4 h

With hydrogen; sulfided platinum; In tetrahydrofuran; ethanol;
DOI:10.1002/jhet.5570240403

Reference yield:

: 112777-35-2
2-methoxy-N-(2-hydroxy-1-methylethyl)-3-aminopyridine

: 112777-44-3
N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-trifuoromethylphenyl)ethanediamide

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

2: tetrahydrofuran / 18 h / Ambient temperature

3: 42 percent / tetrahydrofuran / 4 h

With sodium hydride; In tetrahydrofuran;
DOI:10.1002/jhet.5570240403