3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)

Base Information

Chemical Name:3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)
CAS No.:112777-36-3
Molecular Formula:C10H16 N2 O2
Molecular Weight:196.249
Hs Code.:
Mol file:112777-36-3.mol

Synonyms:3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)

Suppliers and Price of 3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)

Chemical Property:

Boiling Point:289.6±30.0 °C(Predicted)
PKA:3.99±0.11(Predicted)
PSA：43.38000
Density:1.076±0.06 g/cm3(Predicted)
LogP:1.61000

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI)

There total 1 articles about 3-Pyridinamine,2-methoxy-N-(2-methoxy-1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20265-38-7
3-amino-2-methoxypyridine

: 112777-36-3
2-methoxy-N-(2-methoxy-1-methylethyl)-3-amino pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 17.8 g / MgSO₄ / benzene / 1) 2 h reflux 2) stirring at room teperature overnight

2: 41 percent / NaBH₄ / ethanol / 16 h / Heating

3: 71 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

With sodium tetrahydroborate; sodium hydride; magnesium sulfate; In tetrahydrofuran; ethanol; benzene;
DOI:10.1002/jhet.5570240403

Reference yield: 55.0%

: 112777-36-3
2-methoxy-N-(2-methoxy-1-methylethyl)-3-amino pyridine

: 79-04-9
chloroacetyl chloride

: 112777-26-1
1-(2-methoxy-1-methylethyl)-1H-pyrido<2,3-b><1,4>oxazine-2(3H)-one

: 112777-27-2
2-chloro-N-(1,2-dihydro-2-oxo-3-pyridinyl)-N-(2-methoxy-1-methylethyl)acetamide

: 112797-19-0
2-chloro-N-(2-methoxy-1-methylethyl)-N-(2-methoxy-3-pyridinyl)acetamide

Guidance literature:: With 4-vinylpyridine polymer; In tetrahydrofuran; for 2h; Heating;
DOI:10.1002/jhet.5570240403

Reference yield:

: 112777-36-3
2-methoxy-N-(2-methoxy-1-methylethyl)-3-amino pyridine

: 112777-45-4
N-(2-methoxy-3-pyridinyl)-N-(2-methoxy-1-methylethyl)-N'-(3-methoxyphenyl)ethanediamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 18 h / Ambient temperature

2: 15 percent / tetrahydrofuran / 4 h

In tetrahydrofuran;
DOI:10.1002/jhet.5570240403