1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

Base Information

Chemical Name:1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil
CAS No.:699002-91-0
Molecular Formula:C₂₈H₂₅IN₂O₅
Molecular Weight:596.421
Hs Code.:

Synonyms:1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

Chemical Property:

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Technology Process of 1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

There total 5 articles about 1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

: 699002-91-0
1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

Guidance literature:: With sodium hydroxide; In ethanol; for 4h; Heating;
DOI:10.1081/NCN-120027813

Reference yield:

: 54-42-2,162239-35-2
5-Iodo-2'-deoxyuridine

: 699002-91-0
1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / Heating

2: pyridine / 3 h / 20 °C

3: 64 percent / sodium hydroxide / ethanol / 4 h / Heating

With pyridine; sodium hydroxide; In ethanol;
DOI:10.1081/NCN-120027813

Reference yield:

: 76-83-5
trityl chloride

: 699002-91-0
1-(5-O-trityl-2-deoxy-β-D-lyxofuranosyl)-5-iodoracil

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / Heating

2: pyridine / 3 h / 20 °C

3: 64 percent / sodium hydroxide / ethanol / 4 h / Heating

With pyridine; sodium hydroxide; In ethanol;
DOI:10.1081/NCN-120027813