Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate

Base Information

Chemical Name:Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate
CAS No.:101039-82-1
Molecular Formula:C29H27IN2O7S
Molecular Weight:674.513
Hs Code.:
Mol file:101039-82-1.mol

Synonyms:Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate

There total 4 articles about Uridine, 2'-deoxy-5-iodo-5'-O-(triphenylmethyl)-, 3'-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 54-42-2,162239-35-2
5-Iodo-2'-deoxyuridine

: 76-83-5
trityl chloride

: 124-63-0
methanesulfonyl chloride

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

Guidance literature:: 5-Iodo-2'-deoxyuridine; trityl chloride; With pyridine; Heating / reflux;

methanesulfonyl chloride; In dichloromethane;

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 15414-61-6
2'-deoxy-5-iodo-5'-O-(triphenylmethyl)uridine

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1081/NCN-120027813

Reference yield:

: 54-42-2,162239-35-2
5-Iodo-2'-deoxyuridine

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 6 h / 45 °C

2: 1.6 g / pyridine / 1.5 h / 25 °C

With pyridine;
DOI:10.1016/j.bmc.2005.07.046