C₄₁H₄₈Si

Base Information

Chemical Name:C₄₁H₄₈Si
CAS No.:1322595-21-0
Molecular Formula:C₄₁H₄₈Si
Molecular Weight:568.918
Hs Code.:

Synonyms:C₄₁H₄₈Si

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Chemical Property of C₄₁H₄₈Si

Chemical Property:

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Technology Process of C₄₁H₄₈Si

There total 9 articles about C₄₁H₄₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1322595-19-6
C₃₆H₃₉Br

: 1066-54-2
trimethylsilylacetylene

: 1322595-21-0
C₄₁H₄₈Si

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201101057

Reference yield:

: 1322595-16-3
C₃₆H₃₉Br

: 1322595-21-0
C₄₁H₄₈Si

Guidance literature:: Multi-step reaction with 2 steps

1: platinum(II) chloride / toluene / 24.08 h / 25 - 90 °C / Inert atmosphere

2: piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine / 12 h / 80 °C / Inert atmosphere

With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; platinum(II) chloride; In toluene;
DOI:10.1002/chem.201101057

Reference yield:

: 1263428-86-9
1-(tert-butyl)-6-methoxynaphthalene

: 1322595-21-0
C₄₁H₄₈Si

Guidance literature:: Multi-step reaction with 6 steps

1: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 12 h / 80 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 24 h / 80 °C / Inert atmosphere

5: platinum(II) chloride / toluene / 24.08 h / 25 - 90 °C / Inert atmosphere

6: piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine / 12 h / 80 °C / Inert atmosphere

With piperidine; pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; boron tribromide; potassium carbonate; triethylamine; triphenylphosphine; platinum(II) chloride; In 1,4-dioxane; ethanol; dichloromethane; water; toluene;
DOI:10.1002/chem.201101057