C₁₈H₂₀ClN₃O

Base Information

Chemical Name:C₁₈H₂₀ClN₃O
CAS No.:1093064-92-6
Molecular Formula:C₁₈H₂₀ClN₃O
Molecular Weight:329.829
Hs Code.:

C<sub>18</sub>H<sub>20</sub>ClN<sub>3</sub>O

Synonyms:C₁₈H₂₀ClN₃O

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Chemical Property of C₁₈H₂₀ClN₃O

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Technology Process of C₁₈H₂₀ClN₃O

There total 5 articles about C₁₈H₂₀ClN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093063-94-5
C₁₆H₁₉N₃

: 79-04-9
chloroacetyl chloride

: 1093064-92-6
C₁₈H₂₀ClN₃O

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1093064-92-6
C₁₈H₂₀ClN₃O

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / 20 - 100 °C

2.1: potassium acetate; bis(pinacol)diborane / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 20 - 100 °C

2.2: 2 h / 20 - 100 °C

3.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 2-Chloroethyl chloroformate / dichloromethane / 4 h / 20 °C

4.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With aluminum (III) chloride; potassium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 2-Chloroethyl chloroformate; triethylamine; bis(pinacol)diborane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1093063-92-3
1-benzyl-4-(4-bromo-phenyl)-4-methyl-piperidine

: 1093064-92-6
C₁₈H₂₀ClN₃O

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate; bis(pinacol)diborane / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 20 - 100 °C

1.2: 2 h / 20 - 100 °C

2.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 2-Chloroethyl chloroformate / dichloromethane / 4 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 °C

With potassium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 2-Chloroethyl chloroformate; triethylamine; bis(pinacol)diborane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dichloromethane; dimethyl sulfoxide;