(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

Base Information

Chemical Name:(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol
CAS No.:220351-92-8
Molecular Formula:C₂₇H₄₄O₃Si₂
Molecular Weight:472.816
Hs Code.:

Synonyms:(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

Suppliers and Price of (2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

Chemical Property:

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Technology Process of (2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

There total 2 articles about (2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 220351-89-3
(2RS,3S)-3-[[(1,1-Dimethylethyl)diphenylsilyl] oxy]-1,4-pentanediol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 220351-92-8
(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

Guidance literature:: With 1H-imidazole; In DMF (N,N-dimethyl-formamide); at 25 ℃; for 2h;

Reference yield:

: 220351-92-8
(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

Guidance literature:

Reference yield: 26.5%

: 220351-92-8
(2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol

: 220351-95-1
(3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl] oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanone

Guidance literature:: (2RS,3S)-5-[[Dimethyl(1,1-dimethylethyl)silyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl] oxy]-2-pentanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.3h;

With triethylamine; In dichloromethane; at 0 ℃;