C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

Base Information

Chemical Name:C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O
CAS No.:234450-38-5
Molecular Formula:C₂₄H₃₆O₅
Molecular Weight:404.547
Hs Code.:

C<sub>12</sub>H<sub>22</sub>O<sub>2</sub>C<sub>10</sub>H<sub>10</sub>O<sub>2</sub>C<sub>2</sub>H<sub>4</sub>O

Synonyms:C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

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Technology Process of C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

There total 20 articles about C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 107-21-1
ethylene glycol

: 363139-97-3
(4aS,5R,6S,8aR)-5-(6-Hydroxy-2,3-dimethoxy-benzyl)-5,6,8a-trimethyl-octahydro-naphthalen-1-one

: 234450-38-5
C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 8h; Heating;
DOI:10.1021/ol016285h

Reference yield:

: 2033-89-8
3,4-dimethoxyphenol

: 234450-38-5
C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

Guidance literature:: Multi-step reaction with 8 steps

1.1: 78 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 17 h / 0 - 20 °C

2.1: N,N,N',N'-tetramethylethylenediamine / pentane; diethyl ether / 1 h / -78 °C

2.2: bromine / pentane; diethyl ether / 3 h / -78 - 0 °C

2.3: hydrochlorid acid / H₂O; methanol / 5 h / 40 °C

3.1: 96 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 3 h / 20 °C

4.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -40 °C

4.2: 97 percent / tetrahydrofuran; hexane / 2 h / -40 - -20 °C

5.1: NaN(TMS)2 / tetrahydrofuran / 0.5 h / -78 °C

5.2: tetrahydrofuran / 1 h / -78 - -55 °C

5.3: 94 percent / tetrahydrofuran / 2 h / -78 - -55 °C

6.1: 77 percent / n-Bu₃SnH; AIBN / toluene / 2 h / Heating

7.1: 98 percent / aq. HCl / methanol / 2.5 h / 40 °C

8.1: 94 percent / p-TsOH / benzene / 8 h / Heating

With hydrogenchloride; n-butyllithium; 2,2'-azobis(isobutyronitrile); N,N,N,N,-tetramethylethylenediamine; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene; pentane; benzene;
DOI:10.1021/ol016285h

Reference yield:

: 133129-56-3
1,2-dimethoxy-4-(methoxymethoxy)benzene

: 234450-38-5
C₁₂H₂₂O₂C₁₀H₁₀O₂C₂H₄O

Guidance literature:: Multi-step reaction with 7 steps

1.1: N,N,N',N'-tetramethylethylenediamine / pentane; diethyl ether / 1 h / -78 °C

1.2: bromine / pentane; diethyl ether / 3 h / -78 - 0 °C

1.3: hydrochlorid acid / H₂O; methanol / 5 h / 40 °C

2.1: 96 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 3 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -40 °C

3.2: 97 percent / tetrahydrofuran; hexane / 2 h / -40 - -20 °C

4.1: NaN(TMS)2 / tetrahydrofuran / 0.5 h / -78 °C

4.2: tetrahydrofuran / 1 h / -78 - -55 °C

4.3: 94 percent / tetrahydrofuran / 2 h / -78 - -55 °C

5.1: 77 percent / n-Bu₃SnH; AIBN / toluene / 2 h / Heating

6.1: 98 percent / aq. HCl / methanol / 2.5 h / 40 °C

7.1: 94 percent / p-TsOH / benzene / 8 h / Heating

With hydrogenchloride; n-butyllithium; 2,2'-azobis(isobutyronitrile); N,N,N,N,-tetramethylethylenediamine; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene; pentane; benzene;
DOI:10.1021/ol016285h